Information card for entry 4003673

Structure parameters

• Formula: C14 H38 I8 N8 O4 Pb3
• Calculated formula: C14 H38 I8 N8 O4 Pb3
• Title of publication: Formamidinium Haloplumbate Intermediates: The Missing Link in a Chain of Hybrid Perovskites Crystallization
• Authors of publication: Petrov, Andrey A.; Fateev, Sergey A.; Khrustalev, Victor N.; Li, Yumao; Dorovatovskii, Pavel V.; Zubavichus, Yan V.; Goodilin, Eugene A.; Tarasov, Alexey B.
• Journal of publication: Chemistry of Materials
• Year of publication: 2020
• a: 40.2 ± 0.008 Å
• b: 45.72 ± 0.009 Å
• c: 4.58 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8418 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.0445
• Weighted residual factors for significantly intense reflections: 0.1014
• Weighted residual factors for all reflections included in the refinement: 0.1036
• Goodness-of-fit parameter for all reflections included in the refinement: 0.849
• Diffraction radiation wavelength: 0.80246 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No