Crystallography Open Database

Information card for entry 4020013

4020012 << 4020013 >> 4020014

Preview

Coordinates	4020013.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H72 I2 N2 Sn2
Calculated formula	C26 H14 I2 N2 Sn2
Title of publication	Absolute Configuration of 2-(Tributylstannyl)pyrrolidine by Anomalous Dispersion X-ray Analysis
Authors of publication	Robert E. Gawley; Sanjay Narayan; David A. Vicic
Journal of publication	Journal of Organic Chemistry
Year of publication	2005
Journal volume	70
Pages of publication	328 - 329
a	16.04 ± 0.06 Å
b	9.16 ± 0.03 Å
c	16.62 ± 0.1 Å
α	90°
β	117.75 ± 0.04°
γ	90°
Cell volume	2162.7 ± 1.7 Å³
Cell temperature	193.1 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for significantly intense reflections	0.097
Weighted residual factors for all reflections included in the refinement	0.144
Goodness-of-fit parameter for all reflections included in the refinement	14.209
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4020013.html