Information card for entry 4021542

Structure parameters

• Formula: C19 H23 N O5
• Calculated formula: C18.966 H23 N O4.595
• Title of publication: Studies on a Total Synthesis of the Microbial Immunosuppresive Agent FR901483
• Authors of publication: Jeffrey E. Kropf; Ivona C. Meigh; Magnus W. P. Bebbington; Steven M. Weinreb
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2006
• Journal volume: 71
• Pages of publication: 2046 - 2055
• a: 6.1368 ± 0.001 Å
• b: 22.711 ± 0.004 Å
• c: 12.799 ± 0.002 Å
• α: 90°
• β: 90.663 ± 0.003°
• γ: 90°
• Cell volume: 1783.7 ± 0.5 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0794
• Residual factor for significantly intense reflections: 0.0671
• Weighted residual factors for significantly intense reflections: 0.1969
• Weighted residual factors for all reflections included in the refinement: 0.207
• Goodness-of-fit parameter for all reflections included in the refinement: 1.096
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No