Information card for entry 4021719

Structure parameters

• Formula: C22 H30 N2 O2 Os
• Calculated formula: C22 H30 N2 O2 Os
• SMILES: [Os]1(=O)(=O)N([C@H]([C@@H](N1C(C)(C)C)c1ccccc1)c1ccccc1)C(C)(C)C.[Os]1(=O)(=O)N([C@@H]([C@H](N1C(C)(C)C)c1ccccc1)c1ccccc1)C(C)(C)C
• Title of publication: New Osmium-Based Reagent for the Dihydroxylation of Alkenes
• Authors of publication: Timothy J. Donohoe; Robert M. Harris; Sam Butterworth; Jeremy N. Burrows; Andrew Cowley; Jeremy S. Parker
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2006
• Journal volume: 71
• Pages of publication: 4481 - 4489
• a: 19.1714 ± 0.0002 Å
• b: 19.1714 ± 0.0002 Å
• c: 23.39 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8596.82 ± 0.17 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0431
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for all reflections: 0.051
• Weighted residual factors for significantly intense reflections: 0.0299
• Weighted residual factors for all reflections included in the refinement: 0.0299
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0711
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No