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Information card for entry 4021797
Preview
Coordinates | 4021797.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H18 Br2 O5 |
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Calculated formula | C22 H18 Br2 O5 |
Title of publication | Investigation into Factors Influencing Stereoselectivity in the Reactions of Heterocycles with Donor-Acceptor-Substituted Rhodium Carbenoids |
Authors of publication | Simon J. Hedley; Dominic L. Ventura; Paulina M. Dominiak; Cara L. Nygren; Huw M. L. Davies |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2006 |
Journal volume | 71 |
Pages of publication | 5349 - 5356 |
a | 20.5888 ± 0.0005 Å |
b | 6.8523 ± 0.0002 Å |
c | 15.1405 ± 0.0003 Å |
α | 90° |
β | 111.949 ± 0.001° |
γ | 90° |
Cell volume | 1981.19 ± 0.08 Å3 |
Cell temperature | 90 ± 0.1 K |
Ambient diffraction temperature | 90 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 5 |
Hermann-Mauguin space group symbol | C 1 2 1 |
Hall space group symbol | C 2y |
Residual factor for all reflections | 0.0186 |
Residual factor for significantly intense reflections | 0.0179 |
Weighted residual factors for significantly intense reflections | 0.045 |
Weighted residual factors for all reflections included in the refinement | 0.0452 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4021797.html
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