Crystallography Open Database

Information card for entry 4021942

4021941 << 4021942 >> 4021943

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Coordinates	4021942.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H39 N2 O5 P
Calculated formula	C24 H39 N2 O5 P
Title of publication	Diastereoselective Synthesis of 2-Amino-4-phosphonobutanoic Acids by Electrophilic Substitution and Tin-Peterson Olefination of Bis-lactim Ethers Derived from cyclo-[L-AP4-D-Val]
Authors of publication	María C. Fernández; Aniana Díaz; Juan J. Guillín; Olga Blanco; María Ruiz; Vicente Ojea
Journal of publication	Journal of Organic Chemistry
Year of publication	2006
Journal volume	71
Pages of publication	6958 - 6974
a	9.3215 ± 0.0002 Å
b	10.8327 ± 0.0002 Å
c	13.7718 ± 0.0002 Å
α	90°
β	106.425 ± 0.001°
γ	90°
Cell volume	1333.88 ± 0.04 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0425
Residual factor for significantly intense reflections	0.0354
Weighted residual factors for significantly intense reflections	0.0939
Weighted residual factors for all reflections included in the refinement	0.0991
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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