Crystallography Open Database

Information card for entry 4022276

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Coordinates	4022276.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	?
Calculated formula	C24 H36 I4 O8
Title of publication	On the 6-Exo Atom Transfer Radical Cyclization Reactions of 3-Butenyl 2-Iodoalkanoates
Authors of publication	Xingang Fang; Hairong Xia; Hui Yu; Xicheng Dong; Minbo Chen; Quanrui Wang; Fenggang Tao; Chaozhong Li
Journal of publication	Journal of Organic Chemistry
Year of publication	2002
Journal volume	67
Pages of publication	8481 - 8488
a	6.395 ± 0.001 Å
b	6.741 ± 0.001 Å
c	17.932 ± 0.004 Å
α	90°
β	98.22 ± 0.02°
γ	90°
Cell volume	765.1 ± 0.2 Å³
Cell temperature	20 K
Ambient diffraction temperature	20 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.035
Weighted residual factors for significantly intense reflections	0.045
Goodness-of-fit parameter for significantly intense reflections	1.92
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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