Information card for entry 4022682

Structure parameters

• Formula: C34 H50 O17
• Calculated formula: C34 H48 O17
• Title of publication: Synthesis of Macrolide-Saccharide Hybrids by Ring-Closing Metathesis of Precursors Derived from Glycitols and Benzoic Acids
• Authors of publication: Marie-Christine Matos; Paul V. Murphy
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2007
• Journal volume: 72
• Pages of publication: 1803 - 1806
• a: 37.875 ± 0.003 Å
• b: 7.1179 ± 0.0005 Å
• c: 6.4111 ± 0.0004 Å
• α: 90°
• β: 90.101 ± 0.001°
• γ: 90°
• Cell volume: 1728.4 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0458
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.1067
• Weighted residual factors for all reflections included in the refinement: 0.1114
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No