Information card for entry 4022745

Structure parameters

• Formula: C33 H50 O2
• Calculated formula: C33 H50 O2
• Title of publication: Preparation of Chiral Cholestanofluorene and Its Electron-Rich Derivatives for Isolation of a Stable Cation-Radical Salt
• Authors of publication: Paromita Debroy; Ruchi Shukla; Sergey V. Lindeman; Rajendra Rathore
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2007
• Journal volume: 72
• Pages of publication: 1765 - 1769
• a: 46.587 ± 0.007 Å
• b: 5.9312 ± 0.0009 Å
• c: 10.3447 ± 0.0015 Å
• α: 90°
• β: 94.075 ± 0.002°
• γ: 90°
• Cell volume: 2851.2 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0487
• Residual factor for significantly intense reflections: 0.0441
• Weighted residual factors for significantly intense reflections: 0.1153
• Weighted residual factors for all reflections included in the refinement: 0.1192
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No