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Information card for entry 4023054
Preview
Coordinates | 4023054.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C35 H30 N O P |
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Calculated formula | C35 H30 N O P |
SMILES | [P@@]1(=O)(N([C@@H](c2ccccc2)[C@H]2C=Cc3ccccc3[C@@]12C)Cc1ccccc1)c1cccc2ccccc12.[P@]1(=O)(N([C@H](c2ccccc2)[C@@H]2C=Cc3ccccc3[C@]12C)Cc1ccccc1)c1cccc2ccccc12 |
Title of publication | Dearomatizing Anionic Cyclization of N-Alkyl-N-benzyl(dinaphthyl)phosphinamides. A Facile Route to γ-(Amino)dihydronaphthalenylphosphinic Acids |
Authors of publication | Gloria Ruiz-Gómez; María José Iglesias; Manuel Serrano-Ruiz; Fernando López-Ortiz |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2007 |
Journal volume | 72 |
Pages of publication | 9704 - 9712 |
a | 39.056 ± 0.0018 Å |
b | 12.115 ± 0.0005 Å |
c | 11.669 ± 0.0005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5521.3 ± 0.4 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 33 |
Hermann-Mauguin space group symbol | P n a 21 |
Hall space group symbol | P 2c -2n |
Residual factor for all reflections | 0.1155 |
Residual factor for significantly intense reflections | 0.0484 |
Weighted residual factors for significantly intense reflections | 0.0853 |
Weighted residual factors for all reflections included in the refinement | 0.1221 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.835 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4023054.html
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