Information card for entry 4023431

Structure parameters

• Formula: C14 H19 N O
• Calculated formula: C14 H19 N O
• Title of publication: Improved Procedure for the Synthesis of Enamine N-Oxides
• Authors of publication: David Bernier; Alexander J. Blake; Simon Woodward
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2008
• Journal volume: 73
• Pages of publication: 4229 - 4232
• a: 9.7311 ± 0.001 Å
• b: 18.404 ± 0.002 Å
• c: 13.957 ± 0.002 Å
• α: 90°
• β: 99.59 ± 0.002°
• γ: 90°
• Cell volume: 2464.6 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.115
• Residual factor for significantly intense reflections: 0.0918
• Weighted residual factors for significantly intense reflections: 0.236
• Weighted residual factors for all reflections included in the refinement: 0.261
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No