Information card for entry 4023714

Structure parameters

• Formula: C32.5 H31 Cl O6
• Calculated formula: C32.5 H31 Cl O6
• Title of publication: Gold(I)-Catalyzed Intermolecular Addition of Carbon Nucleophiles to 1,5- and 1,6-Enynes
• Authors of publication: Catelijne H. M. Amijs; Verónica López-Carrillo; Mihai Raducan; Patricia Pérez-Galán; Catalina Ferrer; Antonio M. Echavarren
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2008
• Journal volume: 73
• Pages of publication: 7721 - 7730
• a: 11.8034 ± 0.0004 Å
• b: 11.8187 ± 0.0004 Å
• c: 12.4275 ± 0.0004 Å
• α: 105.1 ± 0.002°
• β: 110.678 ± 0.002°
• γ: 107.991 ± 0.002°
• Cell volume: 1403.31 ± 0.08 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0527
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.1206
• Weighted residual factors for all reflections included in the refinement: 0.1286
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No