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Information card for entry 4023970
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Coordinates | 4023970.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C15 H17 Cl O2 |
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Calculated formula | C15 H17 Cl O2 |
Title of publication | Organocatalytic Sequential One-Pot Double Cascade Asymmetric Synthesis of Wieland-Miescher Ketone Analogues from a Knoevenagel/Hydrogenation/Robinson Annulation Sequence: Scope and Applications of Organocatalytic Biomimetic Reductions |
Authors of publication | Dhevalapally B. Ramachary; Mamillapalli Kishor |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2007 |
Journal volume | 72 |
Pages of publication | 5056 - 5068 |
a | 21.065 ± 0.011 Å |
b | 5.735 ± 0.003 Å |
c | 24.155 ± 0.013 Å |
α | 90° |
β | 108.357 ± 0.008° |
γ | 90° |
Cell volume | 2770 ± 3 Å3 |
Cell temperature | 298 ± 2 K |
Ambient diffraction temperature | 298 ± 2 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.074 |
Residual factor for significantly intense reflections | 0.0515 |
Weighted residual factors for significantly intense reflections | 0.1197 |
Weighted residual factors for all reflections included in the refinement | 0.1319 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4023970.html
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