Crystallography Open Database

Information card for entry 4024230

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Coordinates	4024230.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H37 F6 N O P Pd S Sb
Calculated formula	C34 H37 F6 N O P Pd S Sb
Title of publication	Synthesis of Novel Enantiopure Biphenyl P,N-Ligands and Application in Palladium-Catalyzed Asymmetric Addition of Arylboronic Acids to N-Benzylisatin
Authors of publication	Hongshan Lai; Zhiyan Huang; Qiong Wu; Yong Qin
Journal of publication	Journal of Organic Chemistry
Year of publication	2009
Journal volume	74
Pages of publication	283 - 288
a	9.5696 ± 0.0003 Å
b	19.2499 ± 0.0005 Å
c	9.8027 ± 0.0002 Å
α	90°
β	104.089 ± 0.001°
γ	90°
Cell volume	1751.47 ± 0.08 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	9
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0272
Residual factor for significantly intense reflections	0.0253
Weighted residual factors for significantly intense reflections	0.0574
Weighted residual factors for all reflections included in the refinement	0.0584
Goodness-of-fit parameter for all reflections included in the refinement	0.998
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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