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Information card for entry 4024908
Preview
Coordinates | 4024908.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H36 O5 Si |
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Calculated formula | C27 H36 O5 Si |
SMILES | [Si](O[C@@]1(C(C[C@H](C1)c1ccccc1)(C(=O)OC)C(=O)OC)c1ccccc1)(C)(C)C(C)(C)C.[Si](O[C@]1(C(C[C@@H](C1)c1ccccc1)(C(=O)OC)C(=O)OC)c1ccccc1)(C)(C)C(C)(C)C |
Title of publication | Switchable Reactions of Cyclopropanes with Enol Silyl Ethers. Controllable Synthesis of Cyclopentanes and 1,6-Dicarbonyl Compounds |
Authors of publication | Jian-Ping Qu; Chao Deng; Jian Zhou; Xiu-Li Sun; Yong Tang |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2009 |
Journal volume | 74 |
Pages of publication | 7684 - 7689 |
a | 10.4978 ± 0.0009 Å |
b | 20.863 ± 0.0018 Å |
c | 12.9367 ± 0.0012 Å |
α | 90° |
β | 109.675 ± 0.002° |
γ | 90° |
Cell volume | 2667.9 ± 0.4 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0898 |
Residual factor for significantly intense reflections | 0.053 |
Weighted residual factors for significantly intense reflections | 0.1212 |
Weighted residual factors for all reflections included in the refinement | 0.1342 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.919 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4024908.html
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