Crystallography Open Database

Information card for entry 4025610

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Coordinates	4025610.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H18 F6 N Sb
Calculated formula	C23 H18 F6 N Sb
Title of publication	Silver- and Gold-Mediated Intramolecular Cyclization to Substituted Tetracyclic Isoquinolizinium Hexafluorostilbates
Authors of publication	Fang Liu; Xiao Ding; Lei Zhang; Yu Zhou; Linxiang Zhao; Hualiang Jiang; Hong Liu
Journal of publication	Journal of Organic Chemistry
Year of publication	2010
Journal volume	75
Pages of publication	5810 - 5820
a	8.6584 ± 0.0007 Å
b	10.3926 ± 0.0008 Å
c	12.331 ± 0.001 Å
α	79.838 ± 0.001°
β	84.145 ± 0.002°
γ	72.619 ± 0.001°
Cell volume	1040.87 ± 0.14 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0422
Residual factor for significantly intense reflections	0.0363
Weighted residual factors for significantly intense reflections	0.0801
Weighted residual factors for all reflections included in the refinement	0.0825
Goodness-of-fit parameter for all reflections included in the refinement	1.009
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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