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Information card for entry 4025610
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Coordinates | 4025610.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H18 F6 N Sb |
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Calculated formula | C23 H18 F6 N Sb |
Title of publication | Silver- and Gold-Mediated Intramolecular Cyclization to Substituted Tetracyclic Isoquinolizinium Hexafluorostilbates |
Authors of publication | Fang Liu; Xiao Ding; Lei Zhang; Yu Zhou; Linxiang Zhao; Hualiang Jiang; Hong Liu |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2010 |
Journal volume | 75 |
Pages of publication | 5810 - 5820 |
a | 8.6584 ± 0.0007 Å |
b | 10.3926 ± 0.0008 Å |
c | 12.331 ± 0.001 Å |
α | 79.838 ± 0.001° |
β | 84.145 ± 0.002° |
γ | 72.619 ± 0.001° |
Cell volume | 1040.87 ± 0.14 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0422 |
Residual factor for significantly intense reflections | 0.0363 |
Weighted residual factors for significantly intense reflections | 0.0801 |
Weighted residual factors for all reflections included in the refinement | 0.0825 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.009 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4025610.html
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Users of the data should acknowledge the original authors of the
structural data.