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Information card for entry 4026102
Preview
Coordinates | 4026102.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H27 N O2 |
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Calculated formula | C24 H27 N O2 |
SMILES | O1[C@]2(C[C@@H]3C([C@@H]3CC2=N[C@@](C1=O)(C)Cc1cccc2c1cccc2)(C)C)C |
Title of publication | Asymmetric Synthesis of α-Methyl-α-Amino Acids via Diastereoselective Alkylation of (1S)-(+)-3-Carene Derived Tricyclic Iminolactone |
Authors of publication | Ta-Jung Lu; Cheng-Kun Lin |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2011 |
Journal volume | 76 |
Pages of publication | 1621 - 1633 |
a | 6.8347 ± 0.0002 Å |
b | 17.1728 ± 0.0005 Å |
c | 17.4137 ± 0.0005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2043.86 ± 0.1 Å3 |
Cell temperature | 297 ± 2 K |
Ambient diffraction temperature | 297 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.053 |
Residual factor for significantly intense reflections | 0.0408 |
Weighted residual factors for significantly intense reflections | 0.1089 |
Weighted residual factors for all reflections included in the refinement | 0.1145 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.994 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4026102.html
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