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Information card for entry 4026106
Preview
Coordinates | 4026106.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C16 H25 N O2 |
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Calculated formula | C16 H25 N O2 |
SMILES | N1=C2[C@@](OC(=O)[C@]1(C)CCC)(C[C@@H]1C([C@@H]1C2)(C)C)C |
Title of publication | Asymmetric Synthesis of α-Methyl-α-Amino Acids via Diastereoselective Alkylation of (1S)-(+)-3-Carene Derived Tricyclic Iminolactone |
Authors of publication | Ta-Jung Lu; Cheng-Kun Lin |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2011 |
Journal volume | 76 |
Pages of publication | 1621 - 1633 |
a | 7.6999 ± 0.0001 Å |
b | 9.8411 ± 0.0002 Å |
c | 20.3544 ± 0.0004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1542.36 ± 0.05 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0409 |
Residual factor for significantly intense reflections | 0.0406 |
Weighted residual factors for significantly intense reflections | 0.1125 |
Weighted residual factors for all reflections included in the refinement | 0.1128 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.053 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4026106.html
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Users of the data should acknowledge the original authors of the
structural data.