Information card for entry 4026334

Structure parameters

• Formula: C25 H37 N O2 S Si
• Calculated formula: C25 H37 N O2 S Si
• Title of publication: Asymmetric Synthesis of cis-2-Aminocyclopropanols by Intramolecular Mannich Addition of Silyloxy Benzyl Carbanions
• Authors of publication: Bo Liu; Chong-Dao Lu
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2011
• Journal volume: 76
• Pages of publication: 4205 - 4209
• a: 11.0459 ± 0.0003 Å
• b: 22.6548 ± 0.0005 Å
• c: 12.0042 ± 0.0003 Å
• α: 90°
• β: 115.116 ± 0.002°
• γ: 90°
• Cell volume: 2719.94 ± 0.13 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1393
• Residual factor for significantly intense reflections: 0.0608
• Weighted residual factors for significantly intense reflections: 0.1128
• Weighted residual factors for all reflections included in the refinement: 0.1309
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No