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Information card for entry 4027510
Preview
Coordinates | 4027510.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H33 N O2 Si |
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Calculated formula | C24 H33 N O2 Si |
SMILES | C(/C=C\[C@@H]1[C@H](CCCN1)O[Si](c1ccccc1)(c1ccccc1)C(C)(C)C)O |
Title of publication | A Divergent Approach to 3-Piperidinols: A Concise Syntheses of (+)-Swainsonine and Access to the 1-Substituted Quinolizidine Skeleton |
Authors of publication | Glenn Archibald; Chih-Pei Lin; Peter Boyd; David Barker; Vittorio Caprio |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2012 |
Journal volume | 77 |
Pages of publication | 7968 - 7980 |
a | 19.6136 ± 0.0012 Å |
b | 7.3535 ± 0.0004 Å |
c | 16.0097 ± 0.001 Å |
α | 90° |
β | 100.394 ± 0.004° |
γ | 90° |
Cell volume | 2271.2 ± 0.2 Å3 |
Cell temperature | 90 ± 2 K |
Ambient diffraction temperature | 90 ± 2 K |
Number of distinct elements | 5 |
Space group number | 5 |
Hermann-Mauguin space group symbol | C 1 2 1 |
Hall space group symbol | C 2y |
Residual factor for all reflections | 0.0401 |
Residual factor for significantly intense reflections | 0.0347 |
Weighted residual factors for significantly intense reflections | 0.0795 |
Weighted residual factors for all reflections included in the refinement | 0.0828 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4027510.html
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