Information card for entry 4027640

Structure parameters

• Formula: C34 H37 N O7 Si
• Calculated formula: C34 H37 N O7 Si
• Title of publication: Total Synthesis of Pactamycin and Pactamycate: A Detailed Account
• Authors of publication: Stephen Hanessian; Ramkrishna Reddy Vakiti; Stéphane Dorich; Shyamapada Banerjee; Benoît Deschênes-Simard
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2012
• Journal volume: 77
• Pages of publication: 9458 - 9472
• a: 8.8316 ± 0.0003 Å
• b: 10.0485 ± 0.0003 Å
• c: 36.6755 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3254.74 ± 0.17 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0322
• Residual factor for significantly intense reflections: 0.0307
• Weighted residual factors for significantly intense reflections: 0.0837
• Weighted residual factors for all reflections included in the refinement: 0.0846
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No