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Information card for entry 4027772
Preview
Coordinates | 4027772.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C15 H12 N2 O3 |
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Calculated formula | C15 H12 N2 O3 |
Title of publication | A Raney-Cobalt-Mediated Tandem Reductive Cyclization Route to the 1,5-Methanoazocino[4,3-b]indole Framework of the Uleine and Strychnos Alkaloids |
Authors of publication | Tristan A. Reekie; Martin G. Banwell; Anthony C. Willis |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2012 |
Journal volume | 77 |
Pages of publication | 10773 - 10781 |
a | 40.6397 ± 0.0006 Å |
b | 7.7179 ± 0.0001 Å |
c | 17.0144 ± 0.0002 Å |
α | 90° |
β | 97.5888 ± 0.0008° |
γ | 90° |
Cell volume | 5289.88 ± 0.12 Å3 |
Cell temperature | 200 K |
Ambient diffraction temperature | 200 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0648 |
Residual factor for significantly intense reflections | 0.0445 |
Weighted residual factors for all reflections | 0.1107 |
Weighted residual factors for significantly intense reflections | 0.1016 |
Weighted residual factors for all reflections included in the refinement | 0.1107 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.9898 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4027772.html
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