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Information card for entry 4027908
Preview
Coordinates | 4027908.cif |
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Original paper (by DOI) | HTML |
Formula | C48 H56 N4 Si2 |
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Calculated formula | C48 H56 N4 Si2 |
Title of publication | Reactions of Large Tetraaza-N,N'-dihydroacenes: Formation of Unexpected Adducts and an Unstable Tetraazahexacene |
Authors of publication | Jens U. Engelhart; Benjamin D. Lindner; Olena Tverskoy; Manuel Schaffroth; Frank Rominger; Uwe H. F. Bunz |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2013 |
Journal volume | 78 |
Pages of publication | 1249 - 1253 |
a | 7.8787 ± 0.0001 Å |
b | 12.8918 ± 0.0001 Å |
c | 21.5552 ± 0.0002 Å |
α | 93.602 ± 0.001° |
β | 94.672 ± 0.001° |
γ | 95.417 ± 0.001° |
Cell volume | 2166.86 ± 0.04 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.107 |
Residual factor for significantly intense reflections | 0.0607 |
Weighted residual factors for significantly intense reflections | 0.1424 |
Weighted residual factors for all reflections included in the refinement | 0.1668 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.008 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4027908.html
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