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Information card for entry 4027956
Preview
Coordinates | 4027956.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H28 Cl2 F N O4 |
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Calculated formula | C28 H28 Cl2 F N O4 |
Title of publication | Phosphine-Catalyzed Synthesis of 3,3-Spirocyclopenteneoxindoles from γ-Substituted Allenoates: Systematic Studies and Targeted Applications |
Authors of publication | Catherine Gomez; Maxime Gicquel; Jean-Christophe Carry; Laurent Schio; Pascal Retailleau; Arnaud Voituriez; Angela Marinetti |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2013 |
Journal volume | 78 |
Pages of publication | 1488 - 1496 |
a | 9.972 ± 0.0003 Å |
b | 10.748 ± 0.0003 Å |
c | 12.86 ± 0.0004 Å |
α | 84.94 ± 0.0017° |
β | 83.24 ± 0.0016° |
γ | 75.82 ± 0.0018° |
Cell volume | 1324.51 ± 0.07 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0776 |
Residual factor for significantly intense reflections | 0.0568 |
Weighted residual factors for significantly intense reflections | 0.1486 |
Weighted residual factors for all reflections included in the refinement | 0.1652 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4027956.html
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