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Information card for entry 4028013
Preview
Coordinates | 4028013.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C26 H27 O8 P |
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Calculated formula | C26 H27 O8 P |
SMILES | P(=O)(OC1=C([C@H](CCC1)[C@@H]1OC(=O)C=C1)C(=O)OC(C)C)(Oc1ccccc1)Oc1ccccc1.P(=O)(OC1=C([C@@H](CCC1)[C@H]1OC(=O)C=C1)C(=O)OC(C)C)(Oc1ccccc1)Oc1ccccc1 |
Title of publication | Catalytic Enantioselective Vinylogous Mukaiyama-Michael Addition of 2-Silyloxyfurans to Cyclic Unsaturated Oxo Esters |
Authors of publication | Xavier Jusseau; Pascal Retailleau; Laurent Chabaud; Catherine Guillou |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2013 |
Journal volume | 78 |
Pages of publication | 2289 - 2300 |
a | 9.041 ± 0.0002 Å |
b | 19.0319 ± 0.0005 Å |
c | 15.9413 ± 0.0013 Å |
α | 90° |
β | 116.538 ± 0.006° |
γ | 90° |
Cell volume | 2454 ± 0.3 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0976 |
Residual factor for significantly intense reflections | 0.0738 |
Weighted residual factors for significantly intense reflections | 0.1876 |
Weighted residual factors for all reflections included in the refinement | 0.2172 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.154 |
Diffraction radiation wavelength | 1.54187 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4028013.html
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