Information card for entry 4028227

Structure parameters

• Formula: C23 H27 N O3 Si
• Calculated formula: C23 H27 N O3 Si
• SMILES: [Si](C[C@H]1N2[C@H](CCC2=O)[C@@H]2O[C@@H](O[C@H]12)c1ccccc1)(C)(c1ccccc1)C
• Title of publication: Asymmetric Approach to Hyacinthacines B1 and B2
• Authors of publication: Paidi Venkatram Reddy; Julien Smith; Anushree Kamath; Hélène Jamet; Amaël Veyron; Peter Koos; Christian Philouze; Andrew E. Greene; Philippe Delair
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2013
• Journal volume: 78
• Pages of publication: 4840 - 4849
• a: 12.493 ± 0.003 Å
• b: 6.4889 ± 0.0013 Å
• c: 13.275 ± 0.003 Å
• α: 90°
• β: 97.91 ± 0.03°
• γ: 90°
• Cell volume: 1065.9 ± 0.4 ų
• Cell temperature: 296 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.097
• Residual factor for significantly intense reflections: 0.08
• Weighted residual factors for significantly intense reflections: 0.1888
• Weighted residual factors for all reflections included in the refinement: 0.213
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No