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Information card for entry 4028335
Preview
Coordinates | 4028335.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C34 H33 O P |
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Calculated formula | C34 H33 O P |
SMILES | P1(O/C(C(=C1C1CC1)c1ccccc1)=C\C(C)C)(c1ccccc1)(c1ccccc1)c1ccccc1 |
Title of publication | Hydroxyphosphinylation Reaction of 3-Cyclopropylideneprop-2-en-1-ones via C-P σ-Bond Cleavage |
Authors of publication | Maozhong Miao; Jian Cao; Xian Huang; Luling Wu |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2013 |
Journal volume | 78 |
Pages of publication | 5999 - 6007 |
a | 9.8264 ± 0.0006 Å |
b | 9.845 ± 0.0006 Å |
c | 14.8604 ± 0.0009 Å |
α | 86.15 ± 0.005° |
β | 71.839 ± 0.006° |
γ | 81.718 ± 0.005° |
Cell volume | 1351.37 ± 0.15 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0645 |
Residual factor for significantly intense reflections | 0.0443 |
Weighted residual factors for significantly intense reflections | 0.0936 |
Weighted residual factors for all reflections included in the refinement | 0.1042 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.03 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4028335.html
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Users of the data should acknowledge the original authors of the
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