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Information card for entry 4028589
Preview
Coordinates | 4028589.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C19 H24 O7 |
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Calculated formula | C19 H24 O7 |
SMILES | O=C1C[C@]2(O)[C@@H](O[C@@H]3OC(O[C@H]23)(C)C)[C@@H](OCc2ccc(OC)cc2)C1 |
Title of publication | Synthesis of cis- and trans-α-l-[4.3.0]Bicyclo-DNA Monomers for Antisense Technology: Methods for the Diastereoselective Formation of Bicyclic Nucleosides |
Authors of publication | Stephen Hanessian; Benjamin R. Schroeder; Bradley L. Merner; Bin Chen; Eric E. Swayze; Punit P. Seth |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2013 |
Journal volume | 78 |
Pages of publication | 9051 - 9063 |
a | 6.0534 ± 0.0001 Å |
b | 9.3596 ± 0.0002 Å |
c | 31.6166 ± 0.0005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1791.31 ± 0.06 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 3 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.036 |
Residual factor for significantly intense reflections | 0.0334 |
Weighted residual factors for significantly intense reflections | 0.0888 |
Weighted residual factors for all reflections included in the refinement | 0.0906 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.06 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4028589.html
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