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Information card for entry 4028803
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Coordinates | 4028803.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C22 H26 N O3 P |
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Calculated formula | C22 H26 N O3 P |
SMILES | P1(=CC(=O)C(NC(=O)OC(C)(C)C)CC1)(c1ccccc1)c1ccccc1 |
Title of publication | Use of Silver Carbonate in the Wittig Reaction |
Authors of publication | Lukas Jedinak; LaToya Rush; Mijoon Lee; Dusan Hesek; Jed F. Fisher; Bill Boggess; Bruce C. Noll; Shahriar Mobashery |
Journal of publication | Journal of Organic Chemistry |
Year of publication | 2013 |
Journal volume | 78 |
Pages of publication | 12224 - 12228 |
a | 14.2596 ± 0.0006 Å |
b | 10.09 ± 0.0004 Å |
c | 15.1424 ± 0.0006 Å |
α | 90° |
β | 114.587 ± 0.002° |
γ | 90° |
Cell volume | 1981.14 ± 0.14 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0344 |
Residual factor for significantly intense reflections | 0.033 |
Weighted residual factors for significantly intense reflections | 0.0868 |
Weighted residual factors for all reflections included in the refinement | 0.0882 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4028803.html
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