Crystallography Open Database

Information card for entry 4028821

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Coordinates	4028821.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H24 N2 O3
Calculated formula	C23 H24 N2 O3
Title of publication	Asymmetric Synthesis of 2-Substituted Oxetan-3-ones via Metalated SAMP/RAMP Hydrazones
Authors of publication	Joanna V. Geden; Benjamin O. Beasley; Guy J. Clarkson; Michael Shipman
Journal of publication	Journal of Organic Chemistry
Year of publication	2013
Journal volume	78
Pages of publication	12243 - 12250
a	11.52756 ± 0.00012 Å
b	11.52756 ± 0.00012 Å
c	58.0386 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	7712.44 ± 0.15 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	96
Hermann-Mauguin space group symbol	P 43 21 2
Hall space group symbol	P 4nw 2abw
Residual factor for all reflections	0.0708
Residual factor for significantly intense reflections	0.0695
Weighted residual factors for significantly intense reflections	0.1554
Weighted residual factors for all reflections included in the refinement	0.1559
Goodness-of-fit parameter for all reflections included in the refinement	1.138
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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