Information card for entry 4028828

Structure parameters

• Chemical name: (<i>E</i>)-1-(2,4-dinitrophenyl)-2-((triisopropylsilyl)methylene)hydrazine
• Formula: C16 H26 N4 O4 Si
• Calculated formula: C16 H26 N4 O4 Si
• SMILES: C(=N\Nc1c(N(=O)=O)cc(N(=O)=O)cc1)/[Si](C(C)C)(C(C)C)C(C)C
• Title of publication: Synthesis of Formylsilanes through Oxidative Cleavage of α-Silyl Glycols
• Authors of publication: Henrik von Wachenfeldt; Daniel Strand
• Journal of publication: Journal of Organic Chemistry
• Year of publication: 2013
• Journal volume: 78
• Pages of publication: 12268 - 12273
• a: 7.935 ± 0.002 Å
• b: 8.125 ± 0.002 Å
• c: 16.481 ± 0.004 Å
• α: 85.89 ± 0.02°
• β: 80.43 ± 0.02°
• γ: 81.21 ± 0.02°
• Cell volume: 1034.3 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1571
• Residual factor for significantly intense reflections: 0.0877
• Weighted residual factors for significantly intense reflections: 0.2251
• Weighted residual factors for all reflections included in the refinement: 0.286
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No