Information card for entry 4029832

Structure parameters

• Formula: C35 H38 Br I S2 Si2
• Calculated formula: C35 H38 Br I S2 Si2
• Title of publication: Synthesis of molecular tripods based on a rigid 9,9'-spirobifluorene scaffold.
• Authors of publication: Valášek, Michal; Edelmann, Kevin; Gerhard, Lukas; Fuhr, Olaf; Lukas, Maya; Mayor, Marcel
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2014
• Journal volume: 79
• Journal issue: 16
• Pages of publication: 7342 - 7357
• a: 10.7599 ± 0.001 Å
• b: 12.9257 ± 0.0012 Å
• c: 14.6771 ± 0.0019 Å
• α: 101.059 ± 0.009°
• β: 109.431 ± 0.009°
• γ: 96.31 ± 0.007°
• Cell volume: 1855.7 ± 0.4 ų
• Cell temperature: 180.15 K
• Ambient diffraction temperature: 180.15 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0346
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0713
• Weighted residual factors for all reflections included in the refinement: 0.0734
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No