Information card for entry 4029872

Structure parameters

• Formula: C16 H24 Si2
• Calculated formula: C16 H24 Si2
• SMILES: c12ccccc1C=C(/C2=C/[Si](C)(C)C)[Si](C)(C)C
• Title of publication: Diisobutylaluminum Hydride Promoted Cyclization of o-(Trimethylsilylethynyl)styrenes to Indenes.
• Authors of publication: Kinoshita, Hidenori; Hirai, Nobuyoshi; Miura, Katsukiyo
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2014
• Journal volume: 79
• Journal issue: 17
• Pages of publication: 8171 - 8181
• a: 8.5758 ± 0.0008 Å
• b: 24.74 ± 0.002 Å
• c: 16.4424 ± 0.0016 Å
• α: 90°
• β: 90.94 ± 0.001°
• γ: 90°
• Cell volume: 3488 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0692
• Residual factor for significantly intense reflections: 0.0572
• Weighted residual factors for significantly intense reflections: 0.1536
• Weighted residual factors for all reflections included in the refinement: 0.1634
• Goodness-of-fit parameter for all reflections included in the refinement: 0.924
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No