Control of the Dual Reactivity (Iminium-Dienamine) of β-Arylmethyl α,β-Unsaturated Aldehydes in Organocatalytic 1,3-Dipolar Cycloadditions with N-Benzoyl C,N-Cyclic Azomethine Imines.
Authors of publication
Izquierdo, Cristina; Esteban, Francisco; Parra, Alejandro; Alfaro, Ricardo; Alemán, José; Fraile, Alberto; Ruano, José Luis García
Journal of publication
The Journal of organic chemistry
Year of publication
2014
Journal volume
79
Journal issue
21
Pages of publication
10417
a
8.36 ± 0.003 Å
b
11.484 ± 0.005 Å
c
14.287 ± 0.006 Å
α
101.26 ± 0.03°
β
95.06 ± 0.02°
γ
90.03 ± 0.03°
Cell volume
1339.8 ± 1 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.2391
Residual factor for significantly intense reflections
0.1017
Weighted residual factors for significantly intense reflections
0.2109
Weighted residual factors for all reflections included in the refinement
0.2637
Goodness-of-fit parameter for all reflections included in the refinement
