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Information card for entry 4030692
Preview
Coordinates | 4030692.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C16 H15 Br F3 N O2 S |
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Calculated formula | C16 H15 Br F3 N O2 S |
Title of publication | Catalyst-free and metal-free electrophilic bromoamidation of unactivated olefins using the N-bromosuccinimide/sulfonamide protocol. |
Authors of publication | Yu, Wesley Zongrong; Chen, Feng; Cheng, Yi An; Yeung, Ying-Yeung |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2015 |
Journal volume | 80 |
Journal issue | 5 |
Pages of publication | 2815 - 2821 |
a | 6.805 ± 0.002 Å |
b | 8.529 ± 0.003 Å |
c | 15.363 ± 0.005 Å |
α | 74.591 ± 0.007° |
β | 89.569 ± 0.008° |
γ | 87.535 ± 0.007° |
Cell volume | 858.8 ± 0.5 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0672 |
Residual factor for significantly intense reflections | 0.0584 |
Weighted residual factors for significantly intense reflections | 0.1577 |
Weighted residual factors for all reflections included in the refinement | 0.164 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.06 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4030692.html
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Users of the data should acknowledge the original authors of the
structural data.