Information card for entry 4030935

Structure parameters

• Formula: C24 H34 N4 Ni O14 S2
• Calculated formula: C24 H34 N4 Ni O14 S2
• Title of publication: Tetraaquabis(pyridine)metal(II) saccharinate tetrahydrate, [M(H~2~O)~4~(py)~2~](sac)~2~ · 4H~2~O ; M = Co, Ni. Crystal structure determination
• Authors of publication: Jovanovski, G.; Naumov, P.; Grupče, O.; Kaitner, B.
• Journal of publication: European Journal of Solid State and Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 35
• Journal issue: 8-9
• Pages of publication: 579 - 590
• a: 8.555 ± 0.0009 Å
• b: 9.001 ± 0.001 Å
• c: 12.123 ± 0.001 Å
• α: 76.704 ± 0.007°
• β: 84.499 ± 0.007°
• γ: 62.993 ± 0.008°
• Cell volume: 809.38 ± 0.15 ų
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for significantly intense reflections: 0.082
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No