Syntheses of Dihydroconduramines (±)-B-1, (±)-E-1, and (±)-F-1 via Diastereoselective Epoxidation of N-Protected 4-Aminocyclohex-2-en-1-ols.
Authors of publication
Brennan, Méabh B; Csatayová, Kristína; Davies, Stephen G.; Fletcher, Ai M.; Green, William D.; Lee, James A.; Roberts, Paul M.; Russell, Angela J.; Thomson, James E.
Journal of publication
The Journal of organic chemistry
Year of publication
2015
Journal volume
80
Journal issue
13
Pages of publication
6609 - 6618
a
16.6322 ± 0.001 Å
b
24.935 ± 0.0011 Å
c
9.3624 ± 0.0004 Å
α
90°
β
98.764 ± 0.005°
γ
90°
Cell volume
3837.5 ± 0.3 Å3
Cell temperature
150 K
Ambient diffraction temperature
150 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.1385
Residual factor for significantly intense reflections
0.0767
Weighted residual factors for all reflections
0.2405
Weighted residual factors for significantly intense reflections
0.1925
Weighted residual factors for all reflections included in the refinement
0.2399
Goodness-of-fit parameter for all reflections included in the refinement
