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Information card for entry 4032052
Preview
Coordinates | 4032052.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C44 H49 O11 Os3 P |
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Calculated formula | C44 H49 O11 Os3 P |
SMILES | c1(c(cccc1)c1c(cc(cc1C(C)C)C(C)C)C(C)C)[P](C1CCCCC1)(C1CCCCC1)[Os]1(C#[O])(C#[O])(C#[O])[Os](C#[O])(C#[O])(C#[O])(C#[O])[Os]1(C#[O])(C#[O])(C#[O])C#[O] |
Title of publication | Osmium(0)-Catalyzed C-C Coupling of Ethylene and α-Olefins with Diols, Ketols, or Hydroxy Esters via Transfer Hydrogenation. |
Authors of publication | Park, Boyoung Y.; Luong, Tom; Sato, Hiroki; Krische, Michael J. |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2016 |
Journal volume | 81 |
Journal issue | 18 |
Pages of publication | 8585 - 8594 |
a | 11.6048 ± 0.0002 Å |
b | 13.5575 ± 0.0002 Å |
c | 15.1224 ± 0.0002 Å |
α | 74.397 ± 0.001° |
β | 75.404 ± 0.001° |
γ | 84.186 ± 0.001° |
Cell volume | 2216.17 ± 0.06 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0229 |
Residual factor for significantly intense reflections | 0.0222 |
Weighted residual factors for significantly intense reflections | 0.0515 |
Weighted residual factors for all reflections included in the refinement | 0.0517 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.004 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4032052.html
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