Information card for entry 4032067

Structure parameters

• Formula: C18.5 H37 N7 O7.5
• Calculated formula: C18.5 H37 N7 O7.5
• Title of publication: Construction of bis-, tris- and tetrahydrazones by addition of azoalkenes to amines and ammonia
• Authors of publication: Semakin, Artem N.; Kokuev, Aleksandr O.; Nelyubina, Yulia V.; Sukhorukov, Alexey Yu; Zhmurov, Petr A.; Ioffe, Sema L.; Tartakovsky, Vladimir A.
• Journal of publication: Beilstein Journal of Organic Chemistry
• Year of publication: 2016
• Journal volume: 12
• Pages of publication: 2471
• a: 14.325 ± 0.002 Å
• b: 12.234 ± 0.002 Å
• c: 29.447 ± 0.005 Å
• α: 90°
• β: 102.398 ± 0.004°
• γ: 90°
• Cell volume: 5040.3 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2222
• Residual factor for significantly intense reflections: 0.0897
• Weighted residual factors for significantly intense reflections: 0.2017
• Weighted residual factors for all reflections included in the refinement: 0.2715
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No