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Information card for entry 4032076
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Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 4032076.cif |
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Original paper (by DOI) | HTML |
Formula | C16 H18 N2 O |
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Calculated formula | C16 H18 N2 O |
Title of publication | Introduction of Quinolines and Isoquinolines onto Nonactivated α-C-H Bond of Tertiary Amides through a Radical Pathway. |
Authors of publication | Okugawa, Naoki; Moriyama, Katsuhiko; Togo, Hideo |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2017 |
Journal volume | 82 |
Journal issue | 1 |
Pages of publication | 170 - 178 |
a | 10.2286 ± 0.0004 Å |
b | 7.4574 ± 0.0003 Å |
c | 18.7761 ± 0.0007 Å |
α | 90° |
β | 102.144 ± 0.003° |
γ | 90° |
Cell volume | 1400.17 ± 0.1 Å3 |
Cell temperature | 173 K |
Ambient diffraction temperature | 173 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0725 |
Residual factor for significantly intense reflections | 0.0585 |
Weighted residual factors for significantly intense reflections | 0.1522 |
Weighted residual factors for all reflections included in the refinement | 0.161 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4032076.html
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