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Information card for entry 4032088
Preview
Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 4032088.cif |
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Original paper (by DOI) | HTML |
Formula | C18 H23 N O4 S |
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Calculated formula | C18 H23 N O4 S |
Title of publication | Gold-Catalyzed Stereoselective Synthesis of Bicyclic Lactams and Ketones from N-Tosylynamidomethyl-Tethered Cyclohexenes. |
Authors of publication | Zhong, Chang-Zhi; Tung, Po-Ting; Chao, Tsung-Han; Yeh, Ming-Chang P |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2017 |
Journal volume | 82 |
Journal issue | 1 |
Pages of publication | 481 - 501 |
a | 9.9926 ± 0.0005 Å |
b | 14.1265 ± 0.0006 Å |
c | 31.0675 ± 0.0015 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 4385.5 ± 0.4 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 5 |
Space group number | 33 |
Hermann-Mauguin space group symbol | P n a 21 |
Hall space group symbol | P 2c -2n |
Residual factor for all reflections | 0.2378 |
Residual factor for significantly intense reflections | 0.0932 |
Weighted residual factors for significantly intense reflections | 0.1816 |
Weighted residual factors for all reflections included in the refinement | 0.2224 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.895 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4032088.html
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