A Palladium-Catalyzed Ullmann Cross-Coupling/Reductive Cyclization Route to the Carbazole Natural Products 3-Methyl-9H-carbazole, Glycoborine, Glycozoline, Clauszoline K, Mukonine, and Karapinchamine A.
Authors of publication
Yan, Qiao; Gin, Emma; Wasinska-Kalwa, Malgorzata; Banwell, Martin G.; Carr, Paul D.
Journal of publication
The Journal of organic chemistry
Year of publication
2017
Journal volume
82
Journal issue
8
Pages of publication
4148 - 4159
a
21.5986 ± 0.0004 Å
b
6.8991 ± 0.00011 Å
c
17.6362 ± 0.0003 Å
α
90°
β
104.596 ± 0.002°
γ
90°
Cell volume
2543.17 ± 0.08 Å3
Cell temperature
150.01 ± 0.1 K
Ambient diffraction temperature
150.01 ± 0.1 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0871
Residual factor for significantly intense reflections
0.0842
Weighted residual factors for significantly intense reflections
0.2124
Weighted residual factors for all reflections included in the refinement
0.2142
Goodness-of-fit parameter for all reflections included in the refinement
