Information card for entry 4032471

Structure parameters

• Formula: C24 H42 O4 Si2
• Calculated formula: C24 H42 O4 Si2
• SMILES: [Si]1(O[Si](OC[C@@H]2[C@@H](O1)[C@H](O)[C@H](c1ccccc1)C2)(C(C)C)C(C)C)(C(C)C)C(C)C.[Si]1(O[Si](OC[C@H]2[C@H](O1)[C@@H](O)[C@@H](c1ccccc1)C2)(C(C)C)C(C)C)(C(C)C)C(C)C
• Title of publication: Diastereoselective Flexible Synthesis of Carbocyclic C-Nucleosides.
• Authors of publication: Maier, Lukáš; Khirsariya, Prashant; Hylse, Ondřej; Adla, Santosh Kumar; Černová, Lenka; Poljak, Michal; Krajčovičová, Soňa; Weis, Erik; Drápela, Stanislav; Souček, Karel; Paruch, Kamil
• Journal of publication: The Journal of organic chemistry
• Year of publication: 2017
• Journal volume: 82
• Journal issue: 7
• Pages of publication: 3382 - 3402
• a: 9.6577 ± 0.0002 Å
• b: 26.6774 ± 0.0005 Å
• c: 10.5938 ± 0.0002 Å
• α: 90°
• β: 109.914 ± 0.002°
• γ: 90°
• Cell volume: 2566.21 ± 0.09 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0501
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.1212
• Weighted residual factors for all reflections included in the refinement: 0.126
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No