Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4032618
Preview
Coordinates | 4032618.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C39 H30 Cl2 O2 |
---|---|
Calculated formula | C39 H30 Cl2 O2 |
Title of publication | Synthesis, Structures, and Photophysical Properties of Optically Stable 1,16-Diphenyl-3,14-diaryl-Substituted Tetrahydrobenzo[5]helicenediol Derivatives: Enantioselective Recognition toward Tryptophan Methyl Esters. |
Authors of publication | Fang, Lei; Li, Meng; Lin, Wei-Bin; Shen, Yun; Chen, Chuan-Feng |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2017 |
Journal volume | 82 |
Journal issue | 14 |
Pages of publication | 7402 - 7409 |
a | 10.233 ± 0.002 Å |
b | 11.859 ± 0.002 Å |
c | 12.572 ± 0.003 Å |
α | 103.61 ± 0.03° |
β | 95.99 ± 0.03° |
γ | 96.67 ± 0.03° |
Cell volume | 1459 ± 0.6 Å3 |
Cell temperature | 173.15 K |
Ambient diffraction temperature | 173.15 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1445 |
Residual factor for significantly intense reflections | 0.1211 |
Weighted residual factors for significantly intense reflections | 0.3053 |
Weighted residual factors for all reflections included in the refinement | 0.3223 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.152 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4032618.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.