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Information card for entry 4032755
Preview
Coordinates | 4032755.cif |
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Original paper (by DOI) | HTML |
Formula | C14.88 H14.76 F3 N2 O3 |
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Calculated formula | C14.879 H14.748 F3 N2 O3 |
Title of publication | Copper-Catalyzed Selective N-Vinylation of 3-(Hydroxyimino)indolin-2-ones with Alkenyl Boronic Acids: Synthesis of N-Vinyl Nitrones and Spirooxindoles. |
Authors of publication | Chen, Chun-Hua; Liu, Qing-Qing; Ma, Xiao-Pan; Feng, Yu; Liang, Cui; Pan, Cheng-Xue; Su, Gui-Fa; Mo, Dong-Liang |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2017 |
Journal volume | 82 |
Journal issue | 12 |
Pages of publication | 6417 - 6425 |
a | 5.158 ± 0.004 Å |
b | 9.565 ± 0.007 Å |
c | 16.058 ± 0.011 Å |
α | 87.872 ± 0.011° |
β | 87.558 ± 0.011° |
γ | 83.708 ± 0.012° |
Cell volume | 786.3 ± 1 Å3 |
Cell temperature | 296.15 K |
Ambient diffraction temperature | 296.15 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0976 |
Residual factor for significantly intense reflections | 0.086 |
Weighted residual factors for significantly intense reflections | 0.2952 |
Weighted residual factors for all reflections included in the refinement | 0.3103 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.358 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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