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Information card for entry 4033067
Preview
Coordinates | 4033067.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H26 O |
---|---|
Calculated formula | C24 H26 O |
SMILES | C1C[C@H]2[C@@]3([C@H](CCC2)C/C(=C\c2ccc(cc2)c2ccccc2)C3)O1 |
Title of publication | Palladium-Catalyzed Cascade Assembly of Tricyclic Spiroethers from Diene-Alcohol Precursors. |
Authors of publication | Lankri, David; Mostinski, Yelena; Tsvelikhovsky, Dmitry |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2017 |
Journal volume | 82 |
Journal issue | 18 |
Pages of publication | 9452 - 9463 |
a | 5.631 ± 0.001 Å |
b | 7.857 ± 0.002 Å |
c | 41.046 ± 0.008 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1816 ± 0.7 Å3 |
Cell temperature | 296 ± 1 K |
Ambient diffraction temperature | 296 ± 1 K |
Number of distinct elements | 3 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0718 |
Residual factor for significantly intense reflections | 0.0654 |
Weighted residual factors for significantly intense reflections | 0.1488 |
Weighted residual factors for all reflections included in the refinement | 0.1528 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.167 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4033067.html
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