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Information card for entry 4033302
Preview
Coordinates | 4033302.cif |
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Original paper (by DOI) | HTML |
Formula | C23 H25 N O5 |
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Calculated formula | C23 H25 N O5 |
SMILES | O(c1cc2c(nc3ccc(cc3c2cc1)C)[C@@H]1O[C@@H]2OC(O[C@@H]2[C@H]1OC)(C)C)C |
Title of publication | Transition-Metal-Free Synthesis of C-Glycosylated Phenanthridines via K<sub>2</sub>S<sub>2</sub>O<sub>8</sub>-Mediated Oxidative Radical Decarboxylation of Uronic Acids. |
Authors of publication | Zhou, Xin; Wang, Peng; Zhang, Li; Chen, Pengwei; Ma, Mingxu; Song, Ni; Ren, Sumei; Li, Ming |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2018 |
Journal volume | 83 |
Journal issue | 2 |
Pages of publication | 588 - 603 |
a | 7.2135 ± 0.0003 Å |
b | 18.9163 ± 0.0008 Å |
c | 7.7262 ± 0.0003 Å |
α | 90° |
β | 109.331 ± 0.001° |
γ | 90° |
Cell volume | 994.82 ± 0.07 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0447 |
Residual factor for significantly intense reflections | 0.0391 |
Weighted residual factors for significantly intense reflections | 0.0921 |
Weighted residual factors for all reflections included in the refinement | 0.0953 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.088 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4033302.html
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Users of the data should acknowledge the original authors of the
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