Crystallography Open Database

Information card for entry 4033791

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Coordinates	4033791.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H23 B2 Cu F8.67 N5
Calculated formula	C22 H23 B2 Cu F8.66667 N5
Title of publication	Copper(II)-Catalyzed Iodinations of Carbazoles: Access to Functionalized Carbazoles.
Authors of publication	Przypis, Lukasz; Walczak, Krzysztof Zdzislaw
Journal of publication	The Journal of organic chemistry
Year of publication	2019
Journal volume	84
Journal issue	4
Pages of publication	2287 - 2296
a	24.3624 ± 0.0004 Å
b	9.6996 ± 0.0001 Å
c	17.2506 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	4076.41 ± 0.11 Å³
Cell temperature	290 ± 2 K
Ambient diffraction temperature	290 ± 2 K
Number of distinct elements	6
Space group number	30
Hermann-Mauguin space group symbol	P n c 2
Hall space group symbol	P 2 -2bc
Residual factor for all reflections	0.0507
Residual factor for significantly intense reflections	0.0466
Weighted residual factors for significantly intense reflections	0.1337
Weighted residual factors for all reflections included in the refinement	0.1393
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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