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Information card for entry 4033812
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Coordinates | 4033812.cif |
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Original paper (by DOI) | HTML |
Common name | 9-phosphatriptycene tris(pentafluorophenyl)borane complex |
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Chemical name | 9-phosphatriptycene tris(pentafluorophenyl)borane complex |
Formula | C37.71 H14.42 B Cl1.42 F15 P |
Calculated formula | C37.711 H14.422 B Cl1.422 F15 P |
Title of publication | Complementary Synthetic Approaches toward 9-Phosphatriptycene and Structure-Reactivity Investigations of Its Association with Sterically Hindered Lewis Acids. |
Authors of publication | Hu, Lei; Mahaut, Damien; Tumanov, Nikolay; Wouters, Johan; Robiette, Raphaël; Berionni, Guillaume |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2019 |
Journal volume | 84 |
Journal issue | 17 |
Pages of publication | 11268 - 11274 |
a | 15.2134 ± 0.0002 Å |
b | 13.9926 ± 0.00017 Å |
c | 16.96049 ± 0.00017 Å |
α | 90° |
β | 98.3027 ± 0.0012° |
γ | 90° |
Cell volume | 3572.62 ± 0.07 Å3 |
Cell temperature | 295 ± 2 K |
Ambient diffraction temperature | 295 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0562 |
Residual factor for significantly intense reflections | 0.0429 |
Weighted residual factors for significantly intense reflections | 0.1133 |
Weighted residual factors for all reflections included in the refinement | 0.1243 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4033812.html
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