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Information card for entry 4034397
Preview
Coordinates | 4034397.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H27 P S3 |
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Calculated formula | C17 H27 P S3 |
Title of publication | Synthesis of <i>S</i>-Alkyl Phosphinocarbodithioates with Switch between P(III) and P(V) Derivatives. |
Authors of publication | Karpus, Andrii; Daran, Jean-Claude; Poli, Rinaldo; Mazières, Stéphane; Destarac, Mathias A.; Manoury, Eric |
Journal of publication | The Journal of organic chemistry |
Year of publication | 2019 |
Journal volume | 84 |
Journal issue | 15 |
Pages of publication | 9446 - 9453 |
a | 7.6112 ± 0.0001 Å |
b | 11.6546 ± 0.0002 Å |
c | 22.0545 ± 0.0004 Å |
α | 90° |
β | 97.261 ± 0.002° |
γ | 90° |
Cell volume | 1940.67 ± 0.06 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 0.14 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0431 |
Residual factor for significantly intense reflections | 0.0426 |
Weighted residual factors for significantly intense reflections | 0.1135 |
Weighted residual factors for all reflections included in the refinement | 0.1143 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.068 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4034397.html
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